Characteristics of TGPGC on Short Micro Packed Capillary Column.

Characteristics of TGPGC on short micro packed capillary column.

Column switching analysis with packed-capillary columns in gas chromatography.

By introducing sequentially connected two packed-capillary columns, a wide range of volatile compounds were successfully separated in gas chromatography. The hyphenation of two packed-capillary columns of 1.0 mm i.d. was accomplished using a conventional 6-port valve, where the temperature of each column was individually controlled in the respective column ovens. These columns were prepared w...

Rapid temperature-programmed separation and retention prediction on a novel packed-capillary column in gas chromatography.

Novel packed-capillary columns for gas chromatography were developed with a thin-wall stainless-steel capillary of 1.0 mm i.d.; and rapid temperature-programmed separations have been carried out after a basic evaluation concerning the compatibility of these columns to the temperature program. With a numerical integration method, the retention of several test analytes during temperature-programm...

A micro-haematocrit for determining the packed cell volume and haemoglobin concentration on capillary blood.

Gruneberg, 1942; Meyerstein, 1942; Smith, 1944; Harris, Gilding, and Smart, 1951 ; Sabine and Nickolai, 1952) and those open at both ends (Gram and Norgaard, 1923; Van Allen, 1925a and b; Guest, 1938 ; Kato, 1938 and 1940; Miller, 1939 Hamre, 1940; Benditt, Straube, and Humphreys, 1946; Shils, Sass, and Goldwater, 1952). All these tubes suffer from drawbacks either in design or method of use. A...

Simultaneous determination of alcohols and ethylene glycol in serum by packed- or capillary-column gas chromatography.

We developed a packed-column chromatographic procedure capable of simultaneous quantitation of methanol, ethanol, isopropanol, acetone, and ethylene glycol. This method was then updated to a rapid, sensitive, wide-bore capillary method. The packed-column system uses direct injection of 1 microL of Na2WO4/H2SO4-deproteinized serum onto a 1.8 m x 2 mm (i.d.) column packed with 80/100 HayeSep R. A...